FESEM History and Principle

 

 

 

 

 

 

 Ernst Ruska (1906-1987)

 Awarded the Nobel prize in 1986

              

        -FESEM Principle

                 - Basic Concepts

                 -Specimen Preparation

 

 



             Ruska (1986)

 

History

FESEM is the acronym for Field Emission Scanning Electron Microscope. It was Ernest Ruska (1906 – 1987) whom in his PhD. thesis mentioned the potential for electrons to be used in a microscope. In 1933 Ruska and Knoll constructed the first electron microscope and in 1935 Knoll wrote the first work describing the concept of a SEM. In 1938 Von Ardenne built a scanning transmission microscope (STEM) adding coils to a transmission electron microscope.

The first SEM used to study a solid surface was described by Zworykin et al (1942) working for the RCA laboratories in the United States. As a practice in the early days the gun was located in the bottom so the specimen chamber and was high enough for the operator but the specimen might fall down the column. A resolution of 50 nm was achieved with this microscope.

The first micrographs showing the striking three-dimensional imaging capability were obtained in Cambridge at the Engineering Department in 1952 by Dennis McMullan who was continuing the work by Ken Sander (both under C. W. Oatley supervision). The next important step was also in Cambridge when Oatley improved the secondary electron detector by adding a scintillator to convert electrons to photons, and let the way for improvement in signal to noise ratio.

Nowdays, three-dimensional features can be observed due to the large Depth of Field available in the FESEM. The addition of energy dispersive X-ray detector combined with digital image processing is a powerful tool in the study of materials, allowing good chemical analysis of the material. The FESEM is a major tool in materials science research and development.